An important intermediate in corticosteroid biogenesis.
Source:Synthetic
Melting Point:
126-129 degrees C
Solubility:
Chloroform, Dichloromethane
Method for Determining Identity:
Proton NMR Spectroscopic and Mass Spectroscopic Analysis.
TLC Conditions:
SiO2; Hexane: Ethyl Acetate; 2:1; Visualized with AMCS and KMnO4; Single Spot; Rf=0.55. Contains 1.5% Methanol.
Optical Rotation:
-54.4 (c=0.2, CHCI3)
Storage and Stability:
May be stored at RT for short-term only. Long-term storage is recommended at -20 degrees C. For maximum recovery of product, centrifuge the original vial prior to removing the cap.
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